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Thus, hydroxycitrate is a barite crystallization modifier capable of suppressing nucleation and irreversibly inhibiting surface growth. The rate of barite growth prior to hydroxycitrate exposure could not be recovered over 12 h after removal of the modifier, indicating that growth was sustainably (and irreversibly) altered by exposure to hydroxycitrate. Moreover, combined microfluidics and atomic force microscopy measurements reveal that hydroxycitrate fully suppresses growth via the formation of a disordered layer on barite surfaces. Through bulk crystallization, time-resolved microscopy, and scattering measurements, we show that hydroxycitrate (a naturally derived small molecule) effectively inhibits barite nucleation. Here, we explore a series of homologous poly(carboxylic acid)s as crystallization inhibitors of barium sulfate (barite), a pervasive and undesirable mineral scale in many industrial processes. It is less common to observe a modifier with only carboxylate functionality inhibit both nucleation and growth. Inhibitors of mineralization are predominantly composed of either phosphate or carboxylate moieties. Control over this phase transformation is often one-dimensional, meaning that modifiers either block nucleation or impede crystal growth.
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